Pilodist Custom designed Fractional Distillation System

PILODIST 104 Versatile Distillation System is designed to offer exceptional performance and flexibility for a wide range of applications. With its two interchangeable column types and advanced control features, it is ideal for solving challenging separation problems and producing high-purity substances. It is a versatile and reliable distillation system that offers exceptional performance and flexibility for a wide range of applications. Its dual column configuration, advanced control features, and safety mechanisms make it an ideal choice for laboratories and industries seeking precise and efficient distillation.

 

PILODIST SP 1000 M Wiped Film Molecular Distillation System is a state-of-the-art wiped film molecular distillation system designed for the purification of thermally sensitive products under vacuum. Its innovative design and advanced features make it ideal for processing high molecular weight and high viscosity organic compounds. It is a versatile and efficient wiped film molecular distillation system that offers exceptional performance for the purification of thermally sensitive products. Its innovative features and advanced design make it an ideal choice for laboratories and industries seeking high-quality distillation results.

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Description

PILODIST 104 Versatile Distillation System Key Features

 

  • Dual Column Configuration: Choose between the concentric-tube-column and wire gauze trickling column for optimal separation based on the nature of your substances.
  • Temperature-Controlled Oil Bath: Gentle distillation is ensured through precise temperature control of the oil bath, preventing thermal degradation of sensitive compounds.
  • Product Circulation: Efficient product circulation enhances distillation efficiency and ensures consistent results.
  • Flexible Operation: Operate under atmospheric pressure or vacuum conditions to accommodate various distillation requirements.
  • Multiple Receiver Options: Choose between a single final receiver or a spider-type automatic fraction collector with six 1-liter receivers for precise fraction collection.
  • Advanced Control: The DCD4001 distillation control device provides comprehensive control over heating, reflux, vacuum, and fraction collection, ensuring accurate and reliable operation.
  • Safety Features: Built-in safety mechanisms safeguard both the equipment and the user.

 

Applications

 

  • Organic Chemistry: Purification of organic compounds, isolation of specific fractions.
  • Pharmaceutical Industry: Production of active pharmaceutical ingredients (APIs), purification of intermediates.
  • Essential Oils: Extraction and purification of essential oils from plant materials.
  • Research Laboratories: Diverse research applications requiring precise distillation.

 

Technical Specifications

 

  • Column Types: Concentric-tube-column and wire gauze trickling column (DN 25)
  • Temperature Control: Precise temperature control of the oil bath
  • Pressure Range: Atmospheric to vacuum
  • Receiver Options: Single final receiver or spider-type automatic fraction collector
  • Control Device: DCD4001 distillation control device
  • Safety Features:
  • Standards:
    ASTM D1120
    ASTM D1160
    ASTM D2892
    ASTM D2892/5236
    ASTM D5236

 

PILODIST SP 1000 M Key Features

 

  • Vertical Double-Mantled Glass Evaporator: Provides efficient heat transfer and clear process visualization.
  • Rotating PTFE Wiper Elements: Ensures a thin, even film of product on the evaporator surface.
  • Short Path Distillation: Minimizes thermal degradation by reducing the distance vapors travel.
  • Temperature Control: Precise temperature control of the evaporator and condenser for optimal distillation.
  • Interchangeable Vessels: Allows for easy switching between feed and residue vessels, eliminating refilling losses.
  • Vacuum Operation: Operates under high vacuum conditions to reduce boiling points without decomposition.
  • Advanced Design: Features a smart design with liquid-heated lines and vessels, eliminating the need for additional heating equipment.

 

Technical Specifications

 

  • Operating Temperature: Up to 200°C (250-350°C upon request)
  • Vacuum: Down to < 1 x 10^-5 Torr abs.
  • Feed Range: Approximately 1000-4000 ml/h (max. 7000 ml/h)
  • Evaporator Surface: ~1000 cm², short path
  • Evaporator Material of Construction: Borosilicate glass/stainless steel 316
  • Feed Vessel: 3000 ml, graduated, heated, interchangeable
  • Residue Receiver: 3000 ml, graduated, heated, interchangeable or GL-45 bottles
  • Distillate Receiver: 2000 ml, graduated
  • Speed Range of Stirrer: 30-1000 rpm
  • Dimensions: 1750 x 2280 x 820 mm
  • Electrical Supply: 6 individual 230V sockets or optional power distribution box for single line supply 230/400V 25A 50/60Hz with CEE 32A plug
Additional Information
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